“…Similarly, in the purification stage, if the removal of matrix material was incomplete (e.g., only partial hemicelluloses were removed), these matrix materials can prevent the coalescence of the microfibril bundles during the drying period and ease the subsequent fibrillation of the material. In addition, transmitting a charge through the process of oxidation (2,2,6,6-tetramethyl-piperidinyl-1-oxyl radical (TEMPO) region-selective oxidation) or adsorption of charged polyelectrolytes (e.g., carboxymethyl cellulose treatment) on the surface of microfibril increases the interfabrillar repulsive forces (Menta et al, 2014). (B-F) TEM micrographs of (B) sugar palm NFC isolated with high-pressure homogenization through 5 passes at 500 MPa, (C) NFC isolated with microfluidization through 15 passes at 150 MPa (Qing et al, 2013), (D) NFC after microgrinding for 6 hours at 1,500 rpm (Qing et al, 2013), (E) bleached frozen pulp after cryocrushing and treatment in a homogenizer (Alemdar and Sain, 2008), and (F) ultrasonication-derived nanocellulose (Zhou et al, 2012).…”