“…5(a), the microstructure throughout the mortar and pestle mixed pellets is characterized by agglomerates of MgO and Nd 2 Zr 2 O 7 surrounded by an interconnecting matrix of MgO and Nd 2 Zr 2 O 7 grains. The large agglomerates of MgO are detrimental to the corrosion resistance of the composite, however, since the MgO agglomerates will hydrate, swell, and cause cracks to form within the pellet eventually causing catastrophic failure [11]. This process also does not produce consistent microstructures, with different batches producing different agglomerate phases, sizes, and distributions.…”