2002
DOI: 10.1103/physrevb.66.184519
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Microstructure and pinning properties of hexagonal-disc shaped single crystallineMgB2

Abstract: We synthesized hexagonal-disc-shaped MgB 2 single crystals under high-pressure conditions and analyzed the microstructure and pinning properties. The lattice constants and the Laue pattern of the crystals from x-ray micro-diffraction showed the crystal symmetry of MgB 2 . A thorough crystallographic mapping within a single crystal showed that the edge and c axis of hexagonal-disc shape exactly matched the ͓1010͔ and the ͓0001͔ directions of the MgB 2 phase. Thus, these well-shaped single crystals may be the be… Show more

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Cited by 21 publications
(10 citation statements)
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“…28,29 Briefly, a 1:1 mixture of Mg and amorphous B powders was well ground and pressed into a pellet. The pellet was put in a BN container and then placed in a high-pressure cell equipped with a graphite heater.…”
Section: Methodsmentioning
confidence: 99%
“…28,29 Briefly, a 1:1 mixture of Mg and amorphous B powders was well ground and pressed into a pellet. The pellet was put in a BN container and then placed in a high-pressure cell equipped with a graphite heater.…”
Section: Methodsmentioning
confidence: 99%
“…For T 10 K, the influence of the small gap is smeared out by the temperature and C p =T fB=B c2 T; . Specific heat measurements have been performed on single crystals of MgB 2 grown under high pressure [7,8] (with typical dimensions of few hundred microns) using an ac technique. This high sensitivity technique is very well adapted to measure C p of very small samples and to carry continuous measurements during field sweeps at a given temperature.…”
mentioning
confidence: 99%
“…Moreover, MgB 2 crystals typically have small critical current densities j c $ 4 Â 10 8 Am À2 (at 4 K and H a ! 0 [9]) emphasizing the small amount of native disorder. Then, the Bragg Glass should occupy the largest part of the H-T phase diagram.…”
mentioning
confidence: 99%