We obtain some estimates on the area of the boundary and on the volume of a certain free boundary hypersurface Σ with nonpositive Yamabe invariant in a Riemannian n-manifold with bounds for the scalar curvature and the mean curvature of the boundary. Assuming further that Σ is locally volume-minimizing in a manifold M n with scalar curvature bounded below by a nonpositive constant and mean convex boundary, we conclude that locally M splits along Σ. In the case that the scalar curvature of M is at least −n(n − 1) and Σ locally minimizes a certain functional inspired by [30], a neighborhood of Σ in M is isometric to ((−ε, ε) × Σ, dt 2 + e 2t g), where g is Ricci flat.2000 Mathematics Subject Classification. Primary 53C42, 53C21; Secondary 58J60.