2006
DOI: 10.1016/j.diamond.2006.08.032
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Modification of detonation nanodiamonds by heat treatment in air

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Cited by 109 publications
(50 citation statements)
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“…"Piranha" water (sulfuric acid and hydrogen peroxide) constitutes an efficient alternative [124]. Air annealing of NDs at 400-450°C leads to the formation of acid functions mainly carboxylic and to the etching of non-diamond carbon [89,125,126]. A quantitative analysis of COOH groups was performed using Boehm titration after acid treatment [127].…”
Section: Oxidation Of Nanodiamondsmentioning
confidence: 99%
“…"Piranha" water (sulfuric acid and hydrogen peroxide) constitutes an efficient alternative [124]. Air annealing of NDs at 400-450°C leads to the formation of acid functions mainly carboxylic and to the etching of non-diamond carbon [89,125,126]. A quantitative analysis of COOH groups was performed using Boehm titration after acid treatment [127].…”
Section: Oxidation Of Nanodiamondsmentioning
confidence: 99%
“…However so far, agglomerates of diamond nanoparticles have been only dispersed down to very small size when mechanical means have been applied or when most of the material is discarded after dispersion and fractionated sedimentation [5]. Although very efficient in producing nanodiamond colloids, mechanical methods always come on the price of contamination with debris from milling beads [6].…”
Section: Introductionmentioning
confidence: 99%
“…This organization can easily cause interactions between adjacent organics and consequent shifts of their “classical” vibration frequencies. In addition, DNDs tend to adsorb water that forms strong hydrogen bonds with the surface organic groups shifting their vibration frequencies .…”
Section: Resultsmentioning
confidence: 99%