In this research paper, Multiwalled carbon nanotubes (MWCNTs) reinforced with Al2024 were ball milled for homogenization of powder. Nanocomposite was developed using MWCNT reinforcement having 0.5%, 1.5%, and 2.5% weight percentage mixed with Al2024 by powder metallurgy technique. Samples were compacted using a hydraulic press and sintered. Further, sintered samples were solutionized by heating at 560º C followed by quenching and ageing, to