1959
DOI: 10.1021/jo01086a615
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Notes- Decyanoethylation of N,N-Bis(2-cyanoethyl)amides

Abstract: NOTESvol. 24 through Filter Cel. To the yellow filtrate was added 550 ml.ether and the mixture was cooled to 5°. On addition of 49.5 ml. (0.62 mole) of 35% aqueous sodium hydroxide solution, yellow solid separated. This was collected, washed with ether, and dried; yield, 41 g. (69.6%), m.p. 136-140°(uncorr.). Thirty-four g. of the crude base was taken up in 170 ml. dilute hydrochloric acid and the resulting liquid was treated with charcoal and filtered through Filter Cel. After cooling the filtrate to 0-5°, co… Show more

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