“…Numerous studies are to be found in the literature based on vibrational spectroscopy techniques, namely Raman (34,39,(61)(62)(63) and Fourier transform infrared (FTIR) (28,34,35,46,50,54,64), X-ray powder diffraction (XRD) (33,50,57,59,(65)(66)(67), X-ray fluorescence (XRF) (37,38,(68)(69)(70), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) (43,55,57,71), scanning electron microscopy (SEM) (15,43,57,(72)(73)(74)(75), nuclear magnetic resonance (NMR) and magnetic resonance imaging (MRI) (15,76), and computational tomography (CT) (77)(78)(79).…”