Purpose Nitrogen loss as ammonia (NH 3) in a waste cocoa pod co-composting process was determined following the addition of three potential chemical amendments that could lower NH 3 loss. Further, amended compost products were assessed for quality and possible phytotoxicity in a pot experiment. Methods Pod borer damaged cocoa pods were co-composted in lab-scale vessels under ambient conditions with double superphosphate, phosphoric acid, and gypsum at 2%, 5% and 1% of fresh weight, respectively. NH 3 emitted during composting was trapped in standard H 2 SO 4 and determined titrimetrically. Composting mixtures were sampled on days 0, 7, 56 and 90 to monitor pH, total C, total N, and C:N ratio. Mature co-composts were incorporated to the soil at 20 t ha −1 and growth response of Chinese cabbage plants (Brassica rapa chinensis) assessed for the phytotoxicity. Results The chemical amendments were ineffective (p > 0.05) in preventing loss of NH 3 but the quality of composting mixtures were significantly (p < 0.0001) improved. The manure compost generated had acceptable parameters (C, 31.2-31.9% and C:N ratio, 9-10:1) and were free from phytotoxicity for soil application as revealed by the response of Chinese cabbage crop. Conclusions Chemical amendments used in the co-composting process mainly modulated pH without any detrimental effects on quality. The results also demonstrated that the NH 3 loss is insignificant from the cocoa waste-composting process. Further studies are required with increased rates of acidifying amendments like phosphoric acid to further augment the quality of cocoa pod composts.