One-Pot Synthesis of Pyrido[2,3-&amp;lt;i&amp;gt;d&amp;lt;/i&amp;gt;]pyrimidines Catalyzed by Bismuth(III)Triflate

Saglam, Deniz; Turgut, Zühal

doi:10.4236/ijoc.2022.121002

IJOC

2022

DOI: 10.4236/ijoc.2022.121002

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One-Pot Synthesis of Pyrido[2,3-<i>d</i>]pyrimidines Catalyzed by Bismuth(III)Triflate

Deniz Saglam¹,

Zühal Turgut²

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Cited by 3 publications

References 41 publications

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Bismuth(III) Triflate, Bi(OTf)_3: Green and Reusable Catalyst for One‐Pot Synthesis of Fused Nitrogen/Oxygen Heterocycle Derivatives

Mehta,

Patil,

Ahmed

et al. 2024

ChemistrySelect

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There is an increasing demand for the development of catalytic reagents that are nontoxic due to the growing environmental concerns in the present organic transformation. Bismuth(III) compounds have significant potential as catalysts for a range of organic synthesis due to their low toxicity, strong Lewis acid catalytic activity, and great flexibility. In this research work, a series of various chemically and pharmacologically important six‐membered fused nitrogen‐/oxygen‐based heterocycle derivatives were efficiently prepared via a one‐pot multicomponent reaction starting from aromatic aldehydes, malononitrile, and barbituric acid in presence of green and reusable Lewis catalyst bismuth(III) triflate, that is, Bi(OTf)3 in EtOH/H2O (1:1) media. Bi(OTf)3 has the additional benefit of being reusable catalyst, ready availability, eco‐friendliness, and easy to handle to obtain corresponding products in excellent yields (83%–94%). Structure of all synthesized products was characterized on the basis of FT‐IR, 1H‐NMR, 13C‐NMR, and ESI–MS analysis.

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Bismuth(III) Triflate, Bi(OTf)_3: Green and Reusable Catalyst for One‐Pot Synthesis of Fused Nitrogen/Oxygen Heterocycle Derivatives

Mehta,

Patil,

Ahmed

et al. 2024

ChemistrySelect

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Review of the Synthesis, Reactions and Pharmaceutical Potential of Pyrido [2,3-d]Pyrimidine Derivatives

Malah

Shamroukh

2023

COC

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Sustainable Green Synthesis of Pyrimidine Derivatives: Review on Multicomponent Synthesis, Catalysts and Techniques

Eid

2024

COS

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“The founder of green chemistry explains how chemicals manufacturing must change to support a sustainable future.” In this review, Green chemistry is considered in the synthesis of heterocycles compounds containing Pyrimidine nuclei using different catalyzes, solvents, and techniques for the synthesis of pyrimidine derivatives that achieve sustainability. The mentioned fused heterocycles are classified according to the type of ring system. The yield of the target molecules reported in the review is given in the reaction's last step.

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One-Pot Synthesis of Pyrido[2,3-<i>d</i>]pyrimidines Catalyzed by Bismuth(III)Triflate

Cited by 3 publications

References 41 publications

Bismuth(III) Triflate, Bi(OTf)_3: Green and Reusable Catalyst for One‐Pot Synthesis of Fused Nitrogen/Oxygen Heterocycle Derivatives

Bismuth(III) Triflate, Bi(OTf)_3: Green and Reusable Catalyst for One‐Pot Synthesis of Fused Nitrogen/Oxygen Heterocycle Derivatives

Review of the Synthesis, Reactions and Pharmaceutical Potential of Pyrido [2,3-d]Pyrimidine Derivatives

Sustainable Green Synthesis of Pyrimidine Derivatives: Review on Multicomponent Synthesis, Catalysts and Techniques

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One-Pot Synthesis of Pyrido[2,3-&lt;i&gt;d&lt;/i&gt;]pyrimidines Catalyzed by Bismuth(III)Triflate

Cited by 3 publications

References 41 publications

Bismuth(III) Triflate, Bi(OTf)3: Green and Reusable Catalyst for One‐Pot Synthesis of Fused Nitrogen/Oxygen Heterocycle Derivatives

Bismuth(III) Triflate, Bi(OTf)3: Green and Reusable Catalyst for One‐Pot Synthesis of Fused Nitrogen/Oxygen Heterocycle Derivatives

Review of the Synthesis, Reactions and Pharmaceutical Potential of Pyrido [2,3-d]Pyrimidine Derivatives

Sustainable Green Synthesis of Pyrimidine Derivatives: Review on Multicomponent Synthesis, Catalysts and Techniques

Contact Info

Product

Resources

About

One-Pot Synthesis of Pyrido[2,3-<i>d</i>]pyrimidines Catalyzed by Bismuth(III)Triflate

Bismuth(III) Triflate, Bi(OTf)_3: Green and Reusable Catalyst for One‐Pot Synthesis of Fused Nitrogen/Oxygen Heterocycle Derivatives

Bismuth(III) Triflate, Bi(OTf)_3: Green and Reusable Catalyst for One‐Pot Synthesis of Fused Nitrogen/Oxygen Heterocycle Derivatives