“…1(b) shows Williamson-Hall plots for the combustion and hydrothermal samples, where the peak broadening is dependent on both crystallite size and microstrain. The Williamson-Hall equation is given by bcos h = Kk/S + 4e sin h, where k is the wavelength of the X-rays (0.154 nm) and b is the full-width at half maximum of the X-ray peak at the Bragg angle h, K is a shape factor taken as 0.9, S is the crystallite size and e is the microstrain [18].…”