Optimization of process parameters for Cr(VI) removal by seed powder of prickly pear (Opuntia ficus-indica L.) fruits using Taguchi method

Abstract

a b s t r a c tHexavalent chromium is one of the most toxic and carcinogenic heavy metals in aqueous solutions. It is widely used for industrial purposes and released into the environment in large quantities. In this study, Taguchi experimental method was applied to optimize the process parameters for the removal of hexavalent chromium ions from aqueous solutions. Adsorption experiments using seed powder of prickly pear (Opuntia ficus-indica L.) fruits as a new low-cost adsorbent were performed in batch reactor. The five selected controllable parameters, each at three levels, were initial pH of solution (pH 0 ), adsorbent dose (m), initial concentration of metal (C 0 ), time of contact (t), and temperature (T). The L 18 orthogonal array experimental design and "the higher-is-better" criterion were selected to determine optimum removal conditions. The data from all experiments were analyzed using signal-to-noise (S/N) ratio and analysis of variance. The obtained results revealed that the initial pH of the solution was the most important parameter contributing to the removal efficiency (82.48%) followed by adsorbent dose (10.21%), and contact time (5.56%). The optimal conditions for chromium(VI) removal were determined at initial pH of 1, adsorbent dose of 6.0 g/L, initial concentration of metal of 30 mg/L, temperature of 55°C, and time of contact of 80 min, and the Cr(VI) removal percentage was 98.24%. A multiple linear regression equation was developed for estimating predicted values.

Flax fiber based semicarbazide biosorbent for removal of Cr(VI) and Alizarin Red S dye from wastewater

“…As the initial pH increased from 2 to 4, the removal % of Cr(VI) ions and ARS dye decreased very sharply and after that it decreased gradually throughout the process at around 20.0% and 15% for Cr(VI) and ARS, respectively. A similar trend was also observed with the removal of hexavalent chromium using other biosorbents including activated carbon developed from date palm seed, invasive biomass Sargassum muticum, chufa corm peels, and walnut hull 58 , 59 .…”

Effects of Different Chenopodium formosanum Parts on Antioxidant Capacity and Optimal Extraction Analysis by Taguchi Method

“…The Taguchi method (TM) omits the statistical theory and calculation part of the experimental design, and directly analyzes the experimental orthogonal table and experimental data, making it easier to understand and apply in the food industry practice. TM has been used to optimize the process of heavy metal extraction [ 28 ], essential oil extraction [ 29 ], ultrafiltration [ 30 ], drying foods [ 31 , 32 ], and baking parameters [ 33 ].…”