Palladium(II)/Copper(II)‐Catalyzed C–H Sulfidation or Selenation of Arenes Leading to Unsymmetrical Sulfides and Selenides

Nishino, Kota; Tsukahara, Shouya; Ogiwara, Yohei; Sakai, Norio

doi:10.1002/ejoc.201900791

Eur J Org Chem

2019

DOI: 10.1002/ejoc.201900791

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Palladium(II)/Copper(II)‐Catalyzed C–H Sulfidation or Selenation of Arenes Leading to Unsymmetrical Sulfides and Selenides

Kota Nishino

Shouya Tsukahara

Yohei Ogiwara³

et al.

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2023

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Synthesis of Asymmetric Diaryl Sulfides via HI-Mediated C(sp²)-H Sulfenylation of Arenes with Sodium Sulfinates

Sun¹,

Ye²,

Mao³

et al. 2023

J. Org. Chem.

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A novel hydroiodic acid-promoted metal-free C-(sp 2 )-H sulfenylation of electron-rich arenes was developed using stable and easy-to-handle sodium sulfinates as sulfur sources. Diverse kinds of asymmetric aryl sulfides were afforded in good yields from various commercially available aromatic substrates under mild conditions. Comprehensive mechanistic experiments demonstrate that RSO 2 SR and RSSR are the key intermediates responsible for the redox process.

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Synthesis of Asymmetric Diaryl Sulfides via HI-Mediated C(sp²)-H Sulfenylation of Arenes with Sodium Sulfinates

Sun¹,

Ye²,

Mao³

et al. 2023

J. Org. Chem.

View full text Add to dashboard Cite

show abstract

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Palladium(II)/Copper(II)‐Catalyzed C–H Sulfidation or Selenation of Arenes Leading to Unsymmetrical Sulfides and Selenides

Cited by 1 publication

References 5 publications

Synthesis of Asymmetric Diaryl Sulfides via HI-Mediated C(sp²)-H Sulfenylation of Arenes with Sodium Sulfinates

Synthesis of Asymmetric Diaryl Sulfides via HI-Mediated C(sp²)-H Sulfenylation of Arenes with Sodium Sulfinates

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Palladium(II)/Copper(II)‐Catalyzed C–H Sulfidation or Selenation of Arenes Leading to Unsymmetrical Sulfides and Selenides

Cited by 1 publication

References 5 publications

Synthesis of Asymmetric Diaryl Sulfides via HI-Mediated C(sp2)-H Sulfenylation of Arenes with Sodium Sulfinates

Synthesis of Asymmetric Diaryl Sulfides via HI-Mediated C(sp2)-H Sulfenylation of Arenes with Sodium Sulfinates

Contact Info

Product

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Synthesis of Asymmetric Diaryl Sulfides via HI-Mediated C(sp²)-H Sulfenylation of Arenes with Sodium Sulfinates

Synthesis of Asymmetric Diaryl Sulfides via HI-Mediated C(sp²)-H Sulfenylation of Arenes with Sodium Sulfinates