2004
DOI: 10.1149/1.1688802
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Particle Precipitation in Connection with KOH Etching of Silicon

Abstract: This paper considers the precipitation of iron oxide particles in connection with the KOH etching of cavities in silicon wafers. The findings presented in this paper suggest that the source to the particles is the KOH pellets used for making the etching solution. Experiments show that the precipitation is independent of KOH etching time, but that the amount of deposited material varies with dopant type and dopant concentration. The experiments also suggest that the precipitation occurs when the silicon wafers … Show more

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Cited by 14 publications
(8 citation statements)
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“…Each sample was sonicated in concentrated hydrochloric acid prior to retrieval and subsequently dipped in HF (10 s) to remove KOH induced particle precipitation. [57] The average surface roughness (Ra) for each case was determined from 3 lm × 3 lm areas. The results show that TMAH and KOH/IPA yield smooth surfaces (Ra = 0.31 nm and 0.45 nm, respectively) with no systematic differences.…”
Section: Anisotropic Etchant/additives Study and Surface Morphologymentioning
confidence: 99%
“…Each sample was sonicated in concentrated hydrochloric acid prior to retrieval and subsequently dipped in HF (10 s) to remove KOH induced particle precipitation. [57] The average surface roughness (Ra) for each case was determined from 3 lm × 3 lm areas. The results show that TMAH and KOH/IPA yield smooth surfaces (Ra = 0.31 nm and 0.45 nm, respectively) with no systematic differences.…”
Section: Anisotropic Etchant/additives Study and Surface Morphologymentioning
confidence: 99%
“…Prior to the introduction into the MBE system, the samples were wet chemically cleaned using diluted HCl, piranha, and diluted HF. Subsequently, a thin silicon oxide layer was created by wet chemical reoxidation in hydrogen peroxide. , …”
mentioning
confidence: 99%
“…(The ratio of etch rates between (100) and (111) planes is ≈600. ) Substrates were subsequently bathed in dilute hydrochloric acid to remove contaminant particles and etched in dilute hydrofluoric acid to remove the nitride layer. This procedure yielded a sufficiently smooth, mirror-like surface on the etched walls.…”
Section: Methodsmentioning
confidence: 99%