“…The clay fraction (Ͻ2 m) in the podzolic soils from the Estibère watershed represents 4 to 20% of the Ͻ2 mm fraction (Remaury, 1999(Remaury, , 2002. XRD analysis of the clay fraction indicated the presence of smectite (showing X-ray characteristics of a Na-smectite: occurrence of 12.5 Å peak on the air-dried pattern, a 17 Å peak on the ethylene glycoled pattern and their disappearance in the heated pattern), illite (10 Å ), mixed layer illite-smectite (intermediate peaks between 10 Å and 12.5 Å ), and chlorite, and to a lesser extent vermiculite (14 Å ) and kaolinite (7 Å ) in the clay fraction.…”