Photoluminescence spectroscopic monitoring in the synthesis of mesoporous materials by microwave-induced heating

Park, S.-E.; Kim, D.S.; Chang, Jong‐San; Kim, W.Y.

doi:10.1016/s0167-2991(98)81001-x

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Cited by 9 publications

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“…Moreover, this method is energy-efficient and economical. Microwave synthesis has been applied successfully for the synthesis of many zeolites and molecular sieves such as A, Y, ZSM-5, Beta, MCM-41, TS-1, aluminophosphates such as AlPO 4 -5, CoAPO-5, MgAPO-5, AlPO 4 -11 and large pore gallophosphate cloverite and GaPO 4 [12][13][14][15][16][17][18][19]. Also mesoporous MCM-41 has been synthesized.…”

Section: Introductionmentioning

confidence: 99%

Synthesis of MCM-48 by microwave-hydrothermal process

Bandyopadhyay

Gies

2005

Comptes Rendus. Chimie

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MCM-48 was synthesized using the microwave hydrothermal method. The material was characterized by means of powder XRD, NMR, sorption measurement, SEM and transmission electron microscopy (TEM). XRD, NMR confirm the topology of the silicate framework, TEM shows the periodicity and homogeneity of the MCM-48 frame structure. However, from TEM it is clear that there is structural disorder. Beside MCM-48 a mesoporous wormhole like structure coexists. This is reflected in the lowering of the surface area and pore volume compared to the conventional, hydrothermally prepared MCM-48 material. To cite this article: M.

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