“…Mn 2+ and Cr 3+ ) [14,15] to prepare phosphors emitting mostly in the visible range of the electromagnetic spectrum. Researchers in this study are particularly interested in the performance of a nanocrystalline ZnAl 2 O 4 because of the speculation that nanocrystalline materials may have better optical properties than their bulk counterparts [11]. Different synthesis methods such as sol-gel [16,17], hydrothermal [18,19], combustion [6,15,20] and solid state reaction [21] are commonly used to prepare rare-earth/transition metal doped nanocrystalline ZnAl 2 O 4 phosphors.…”