A conductometric H 2 , NO 2 , and hydrocarbon gas sensor based on single-crystalline zinc oxide (ZnO) nanobelts has been developed. The nanobelt sensitive layer was deposited using a radio frequency (RF) magnetron sputterer. The microcharacterization study reveals that the nanobelts have a single crystal hexagonal structure with average thickness and width of about 10 and 50 nm, respectively. The sensor was exposed to H 2 , NO 2 and propene gases at operating temperatures between 150 C and 450 C. The study showed that optimum operating temperatures for the sensor are in the range of 300 C-400 C for H 2 , 300 C-350 C for NO 2 , and 350 C-420 C for propene sensing.