2009
DOI: 10.1007/s10971-009-1992-4
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Porous structure of polybenzoxazine-based organic aerogel prepared by sol–gel process and their carbon aerogels

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Cited by 123 publications
(99 citation statements)
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“…The second peak, appeared at 500 • C once the air was introduced and represents the combustion of the char. Lorjai et al [13] used thermogravimetric analysis to investigate the thermal degradation of polybenzoxazine. They pointed out that polybenzoxazine began to lose weight at 250 • C, and the highest maximum mass loss rate was observed in the temperature range of 250-600 • C. Hung et al [14] studied the thermal degradation of pure phenolic resin by TGA from room temperature to 800 • C with a heating rate of 10 • C min −1 under nitrogen atmosphere.…”
Section: Resultsmentioning
confidence: 99%
“…The second peak, appeared at 500 • C once the air was introduced and represents the combustion of the char. Lorjai et al [13] used thermogravimetric analysis to investigate the thermal degradation of polybenzoxazine. They pointed out that polybenzoxazine began to lose weight at 250 • C, and the highest maximum mass loss rate was observed in the temperature range of 250-600 • C. Hung et al [14] studied the thermal degradation of pure phenolic resin by TGA from room temperature to 800 • C with a heating rate of 10 • C min −1 under nitrogen atmosphere.…”
Section: Resultsmentioning
confidence: 99%
“…The polybenzoxazine precursors were prepared by mixing bisphenol-A, TETA, and formaldehyde at a mole ratio of 1:1:4, respectively [6,7]. Firstly, bisphenol-A (6.84 g, 30 mmol) was dissolved in 1,4-dioxane (15 mL) in a 50 mL glass bottle and was stirred until a clear solution was obtained.…”
Section: Synthesis Of Polybenzoxazinementioning
confidence: 99%
“…In addition, polybenzoxazine is a cross-linked polymer with additional extensive hydrogen bonded networks which can withstand pore collapse without the need of supercritical CO 2 drying process. Hence, polybenzoxazine aerogels with more economical ambient drying have been reported in the literature [35][36][37][38][39][40][41][42].…”
Section: Introductionmentioning
confidence: 99%
“…In 2009, polybenzoxazine-based carbon aerogels were first introduced by Lorjai et al who found that their carbon aerogel exhibited the properties as a microporous material [35]. In 2010, polybenzoxazine-based carbon aerogels with an average pore diameter of 3.67 nm were used as an electrode in supercapacitors by Katanyoota et al [36].…”
Section: Introductionmentioning
confidence: 99%