“…Several copper meshes coated with carbon were previously placed on the aluminum foils to collect the fiber samples for transmission electron microscope (TEM) analysis. In this work, the electrospun pure SF fibers were also prepared as described previously for comparison [29].…”
“…Several copper meshes coated with carbon were previously placed on the aluminum foils to collect the fiber samples for transmission electron microscope (TEM) analysis. In this work, the electrospun pure SF fibers were also prepared as described previously for comparison [29].…”
“…This composite material was developed to improve the structure and mechanical property of the regenerated silk by sericin [72]. In a similar research, sericin enhanced the electrospinnability of the regenerated silk fibroin blend to produce high-quality regenerated silk materials used in medical field [73].…”
Section: Regenerated Keratin Fibers and Compositesmentioning
Introduction Definition Biopolymers are defined as macromolecules completely or partially produced in a normal way by living organisms [1]. The prefix "bio" means that they are produced by living organisms and thus are biodegradable.
“…The B. mori cocoons were boiled twice in 0.5 wt% Na 2 CO 3 solution to remove sericin. Degummed silks were then dissolved in 9.0 M LiBr aqueous solution at 40 ∘ C for 2 h and further dialyzed in deionized water at 10 ∘ C for 3 days according to the established procedures [19]. Ultimately, a purified 33 wt% SF solution was obtained through concentrating at 10 ∘ C.…”
Section: Preparation Of Silk Fibroin and Electrospunmentioning
Regenerated silk fibroin (SF) mats were fabricated using electrospinning technique, followed by mild water vapor annealing to effectively tune the structures and improve the mechanical properties of the mats at different annealing times and temperatures. The breaking strength and the breaking energy of the mats treated with water vapor at 65°C for 12 h reached 6.0 MPa and 171.7 J/kg, respectively. The conformational transition of the SF mats was significantly influenced by the treating temperature, while the influence of time was comparatively limited. The influence is consistent with the time-temperature equivalent principle and would be helpful for the preparation of water-vapor-annealed silk-based biomaterials for various applications.
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