Turbulent flow and ozone concentration at two (rooftop and sidewalk) sites in a high-rise building area of Seoul, Republic of Korea, were measured for the period of 24−27 June 2013 to examine their characteristics according to site location. During the observation period, the diurnal variations of air temperature, wind speed, and turbulent kinetic energy were distinct at both sites. The time series of ozone concentration exhibits a diurnal variation with daytime double peaks and one nighttime peak at both sites. The horizontal wind direction at the rooftop site has variations related to local winds, while the horizontal wind direction at the sidewalk site is mostly southerly (following a nearby street). The multiresolution spectra of horizontal and vertical velocities at the rooftop site confirm diurnal and turbulence-related variations. A quadrant analysis indicates that turbulence at the rooftop site is characterized by frequent ejections and less frequent but stronger sweeps, while turbulence at the sidewalk site is weaker and less characterizable than turbulence at the rooftop site.