“…Several studies have reported the utilization of natural-made fillers: Expanded vermiculite [45], pumice [40], lightweight expanded clay aggregate (LECA) [3,46], expanded perlite (EP) [47,48] and expanded glass (EG) [2,49]. In other cases, commercial or human-made lightweight aggregates have been successfully used: fly-ash cenospheres (FAC) [50][51][52], glass microballoons (GMB) [1,5], ceramic spheres (CMB) [11,53,54], carbon hollow spheres [55] and hollow metallic spheres [56]. Pores can contain traces of various gases like CO 2 , N 2 , H 2 O, CO and O 2 [57] as a result of fillers manufacturing methods.Apart from these two physical properties of reinforcements (chemical compositions and inner nature), there are several properties that must be controlled to optimize characteristics such as porosity (thickness-to-size ratio, shell porosity, compressive collapse strength, shrinkage and melting temperature) and wettability (surface roughness, coating properties and interface chemical reactions).In terms of size, Puga et al [3] observed that porous nature brittle fillers (such as LECA) tend to increase MMSF yield strength whilst fillers size and density increases and decreases respectively.…”