2015
DOI: 10.1016/j.chroma.2015.01.033
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Rapid analysis of pharmaceuticals and personal care products in fish plasma micro-aliquots using liquid chromatography tandem mass spectrometry

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Cited by 38 publications
(7 citation statements)
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“…After the fish were exposed, fish blood samples were collected by tail cutting, as described previously by Chen et al 36 . The tail of each fish was cut off using sterilized spring scissors to expose the caudal vein.…”
Section: Methodsmentioning
confidence: 99%
“…After the fish were exposed, fish blood samples were collected by tail cutting, as described previously by Chen et al 36 . The tail of each fish was cut off using sterilized spring scissors to expose the caudal vein.…”
Section: Methodsmentioning
confidence: 99%
“…Widely used human drugs such as rantidine, fluoxetine, ibuprofen, caffeine, diphenhydramine, propranolol and statins were added to the screening protocol and assessed. Other drugs, including carbamazepine, diltiazem, and gemfibrozil which are commonly found in effluents and have been found to accumulate in fish (Ramirez et al 2007;Chen et al 2015;Meador et al 2016) were also included.…”
Section: Selection Of New Analytesmentioning
confidence: 99%
“…The aim of this work was to assess the ability of this method to screen for additional classes of compounds beyond those included in the original method for veterinary drug residues (Turnipseed et al 2017) including triazine herbicides, organophosphate and carbamate pesticides, human pharmaceuticals, selected disinfectants, growth promoters and some newer antibiotics. While other published LC-MS methods are available for monitoring aquaculture or wild fish for chemical contaminants including pesticides (Han et al 2014;Song et al 2018) or pharmaceuticals and personal care products (Ramirez et al 2007;Chen et al 2015), the goal of this study was to determine how well representative compounds that may be found in fish can be detected in a single HRMS screening method. Spikes of all compounds were made at levels of 100, 10 and 1 ng/g to test method performance and determine confirmatory screening limits for each added compound.…”
Section: Introductionmentioning
confidence: 99%
“…Owing to the large-scale dilution of these contaminants in water sources (natural waters) or due to the matrix complexity, a preliminary sample preparation technique for concentration or/and clean-up is mandatory, such as liquid-liquid extraction (LLE) [57], solid-phase extraction (SPE) [10,27,[58][59][60], solid-phase microextraction (SPME) [27,28], or stir bar sorptive extraction (SBSE) [61]. Currently, pharmaceuticals are usually extracted from water samples by off-line solid-phase extraction [10,46,61] and on-line solid phase extraction [44,62].…”
Section: Introductionmentioning
confidence: 99%