Rapid determination of polycyclic aromatic hydrocarbons in grilled meat using microwave-assisted extraction and dispersive liquid–liquid microextraction coupled to gas chromatography–mass spectrometry

Kamankesh, Marzieh; Mohammadi, Abdorreza; Hosseini, Hedayat; Tehrani, Z. Modarres

doi:10.1016/j.meatsci.2015.01.001

Cited by 91 publications

(36 citation statements)

References 38 publications

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“…Sample pH and extraction volume were selected according to our previous study (15)(16)(17). pH 7 and 500 µL chloroform were used for all experiments.…”

Section: Resultsmentioning

confidence: 99%

Determining the amount of Acrylamide in Potato Chips Using Xanthydrol as a Derivative Representative with Gas Chromatography-Mass Spectrometry

et al. 2016

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A B S T R A C T Background and Objectives:In the production process of foods rich in carbohydrates and some other foods containing precursors of acrylamide formation, there is the possibility of acrylamide creation, which is a mutagen and carcinogen material. This study aims to introduce and optimize a new method for determining acrylamide in potato chips using xanthydrol as a derivative representative with gas chromatography-mass spectrometry. Materials and Methods:Important factors in the derivatization and measurement processes were optimized using the one-factor-at-a-time method. The peak areas were assumed as the GC-MS response to evaluate the extraction efficiency of acrylamide, and optimization for all tests was performed two times. Figures of merit of the proposed method were evaluated. The amount of acrylamide in four potato chips samples, obtained from the market in Tehran city, was determined using the proposed method. Results:The optimum amounts of effective parameters, including derivatization temperature at 25 o C, derivatization time (40 min), xanthydrol volume (40 µL), extracted solvent volume (500 µL) and pH=7 were determined. The figures of merit for the proposed method were at the ideal range. The maximum and minimum amounts of acrylamide in the chip samples were also measured. Conclusions:The performance and reliability of proposed method as a simple, efficient and rapid method for determining acrylamide in potato chip samples were demonstrated.

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“…Sample pH and extraction volume were selected according to our previous study (15)(16)(17). pH 7 and 500 µL chloroform were used for all experiments.…”

Section: Resultsmentioning

confidence: 99%

Determining the amount of Acrylamide in Potato Chips Using Xanthydrol as a Derivative Representative with Gas Chromatography-Mass Spectrometry

et al. 2016

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“…The liquid smoke used in the conducted experiments was analysed using the same GC-MS as mentioned above and according to the recommended temperature program (10): fi rst at 150 °C for 2 min and then the temperature was increased by 7 °C/min to 200 °C, held for 1 min, and then increased by 5 °C/min to 250 °C and held for 1 min. Finally, it was increased rapidly by 20 °C/min to 290 °C and kept for 10 min.…”

Section: Determination Of Liquid Smoke Chemical Compositionmentioning

confidence: 99%

“…Liquid smoke application has been increasingly widespread as a suitable replacer for traditional wood smoking due to several advantages, such as more effi cient control of polycyclic aromatic hydrocarbon (PAH) content, in which their constituents can be determined by rapid methods (10), bett er applicability to diff erent food systems and lower environmental pollution (11).…”

Section: Introductionmentioning

confidence: 99%

The Anti-Staphylococcus aureus Effect of Combined Echinophora platyloba Essential Oil and Liquid Smoke in Beef

Pilevar

Hosseini

Hajimehdipoor

et al. 2017

Food Technol. Biotechnol.

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“…Their significant toxicity, potential mutagenicity and carcinogenicity enable them as priority pollutants in the European Union and U.S.Environment Protection Agencies [7][8][9]. Many studies have already been conducted for preconcentration and determination of PAH S by solid phase extraction (SPE) [10][11][12], solid phase microextraction (SPME) [13][14][15], and dispersive liquid-liquid microextraction (DLLME) [16][17][18].…”

Section: Introductionmentioning

confidence: 99%

The headspace solid-phase microextraction of polycyclic aromatic hydrocarbons in environmental water samples using silica fiber modified by self assembled gold nanoparticles

2015

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The headspace solid phase microextraction method with modified silica fibers prepared based on self assembled gold nanoparticles and sol-gel method is described for the determination of trace amount of polycyclic aromatic hydrocarbons in environmental water samples using high performance liquid chromatography-UV detection. Extraction parameters such as extraction time, extraction temperature, desorption time, type and volume of desorption solvent, sample volume and ionic strength were evaluated and optimized by experimental design. At optimum specified conditions, high characteristic performance such as reproducibility and repeatability and linear range (1-500 ng mL -1 ) along the reasonable determination coefficient up to 0.995, presence of low limit of detection (from 0.10 to 0.89 ng mL -1 ) suggest good and efficient applicability of method for estimation and quantification of understudy analytes. The proposed method was successfully applied for the extraction of polycyclic aromatic hydrocarbons in various environmental samples with relative recoveries for the spiked samples at 50 ng mL -1 of analytes in the range of 84 to 106% and RSDs below 5.1%. Also, reproducibility of fiber were in the range of 1.2-3.9, reproducibility of proposed fiber were in the range of 3.6-6.7.

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Rapid determination of polycyclic aromatic hydrocarbons in grilled meat using microwave-assisted extraction and dispersive liquid–liquid microextraction coupled to gas chromatography–mass spectrometry

Cited by 91 publications

References 38 publications

Determining the amount of Acrylamide in Potato Chips Using Xanthydrol as a Derivative Representative with Gas Chromatography-Mass Spectrometry

Determining the amount of Acrylamide in Potato Chips Using Xanthydrol as a Derivative Representative with Gas Chromatography-Mass Spectrometry

The Anti-Staphylococcus aureus Effect of Combined Echinophora platyloba Essential Oil and Liquid Smoke in Beef

The headspace solid-phase microextraction of polycyclic aromatic hydrocarbons in environmental water samples using silica fiber modified by self assembled gold nanoparticles

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