Rapid micromethods of elemental analysis. III. Precise conlometric determination of hydrogen in organic compounds

Electroanalysis and Coulometric Analysis

“…Several papers were concerned with the determination of water by adsorption on a P206 film and subsequent electrolysis between platinum electrodes (198,247). A similar technique was used for the determination of hydrogen in organic compounds (9,193,246). By using this technique, 3-mg. samples containing about 3.2% hydrogen could be determined with a standard deviation of between 0.01 and 0.03%.…”