1974
DOI: 10.1021/ac60339a028
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Separations on heavily loaded small particle columns in high speed liquid chromatography

Abstract: cedure is preferred since a complete base-line separation is not required. However, the type of accuracy and reproducibility obtained will be a function of the ability to control and reproduce the flow properties and sample injection procedure. No attempt was made to use an internal standard technique or electronic integration.Samples 3 and 4 in Table III illustrate how different eluting conditions can be used for the same separation. In sample 3, a higher pH and lower alcohol concentration is used. At this co… Show more

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Cited by 90 publications
(6 citation statements)
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“…Liquid-liquid partition chromatography on heavily-loaded silica columns was studied (116,483). COLUMN TECHNIQUES Ion-Pair Partition Chromatography.…”
Section: Nonchromatographic Uses Of Resins and Absorbentsmentioning
confidence: 99%
“…Liquid-liquid partition chromatography on heavily-loaded silica columns was studied (116,483). COLUMN TECHNIQUES Ion-Pair Partition Chromatography.…”
Section: Nonchromatographic Uses Of Resins and Absorbentsmentioning
confidence: 99%
“…Amino acid derivatives are more amenable to separation by non-ionic chromatography, and major emphasis has been given to the phenylthiohydantoin derivatives, which have been separated both by normal and reverse-phase methods (281-286). Separation of dansyl amino acids has also been reported (187).…”
mentioning
confidence: 99%
“…For silica supports, coated with 3,3'-oxydipropionitrile (4), water (5), or formamid (5) and eluted with hexane or dichloromethane, pronounced influence from the support on the retention was observed for polar uncharged compounds and even at high loadings. The same observation was made with organic ammonium ions on silica columns coated with buffer and eluted with chloroform + 1-pentanol (3), but the support interaction was small at the maximal loading of the buffer.…”
mentioning
confidence: 99%