“…[4] Co 3 O 4 , which has the typical spinel structure of a transition metal oxide, has been used as a support for noble metals in the activation of hydrocarbons. [5][6][7][8] A variety of different methods have been developed for the preparation of cobalt oxide nanoparticles, including the sol-gel, [9] microwave-assisted, [10] chemical vapor deposition, [11][12][13][14] chemical precursor route, [14] electrochemical synthesis, [15,16] spray pyrolysis, [17] and a simple reduction oxidation [18] methods. It is well known that the behaviors of nanophase materials are strongly dependent on the shapes and sizes of the particles, and the control of these properties is therefore critical to the ultimate performance and application of these materials.…”