“…Microextraction and selective adsorption procedures can also be considered to enhance TXRF microanalytical capability. For instance in the case of Se and Hg determination of low level (0.6 g L −1 ) in seafood samples 110 and in the determination of Sb in milk after nanoparticles immobilization reflectors, 111 respectively.…”
The need for elemental analysis in quality control of food, pharmaceuticals and cosmetics, taking into account human safety, has become an essential requirement for any product destinated for commercialization and...
“…Microextraction and selective adsorption procedures can also be considered to enhance TXRF microanalytical capability. For instance in the case of Se and Hg determination of low level (0.6 g L −1 ) in seafood samples 110 and in the determination of Sb in milk after nanoparticles immobilization reflectors, 111 respectively.…”
The need for elemental analysis in quality control of food, pharmaceuticals and cosmetics, taking into account human safety, has become an essential requirement for any product destinated for commercialization and...
“…A report by Romero et al 66 described the trapping of Hg and Se vapours using silver NPs immobilised on quartz reectors prior to their determination by TXRF spectrometry. A report by Romero et al 66 described the trapping of Hg and Se vapours using silver NPs immobilised on quartz reectors prior to their determination by TXRF spectrometry.…”
Section: Txrf and Related Techniquesmentioning
confidence: 99%
“…The analysis of nanoparticles (NPs) is of growing interest. A report by Romero et al 66 described the trapping of Hg and Se vapours using silver NPs immobilised on quartz reectors prior to their determination by TXRF spectrometry. The authors described in detail how the quartz reectors were prepared and how the NPs were immobilised on the surface.…”
This review covers developments in and applications of XRF techniques such as EDXRF, WDXRF, TXRF, XRF microscopy using technologies such as synchrotron sources, X-ray optics, X-ray tubes and detectors in laboratory, mobile and hand-held systems.
“…[25][26][27][28] Some applications of silver nanoparticles (AgNPs) for the determination of mercury or its removal from contaminated water have been reported. Romero et al 29 used the procedure of trapping Hg vapours using AgNPs immobilized on quartz reectors, prior to their determination by total reection X-ray uorescence. Panichev et al 30 proposed silver and gold nanoparticles impregnated in nylon membrane lters as a new solid phase for preconcentration of mercury from natural waters.…”
In this study, the analytical potential of USA DMSPE with silver nanoparticles as a solid sorbent combined with high-resolution continuum source ETAAS in the determination of mercury was evaluated.
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