“…This phase transition is associated with abrupt changes in optical and electrical properties; therefore, VO has potential applications, for example, in preparing thermal and optical switches (2,3). Although various technologies have been developed for producing VO "lms (4,5), few convenient ones have been found for making VO powders. The typical method of preparing VO powders is to heat a mixture of V O (or V) and V O corresponding to VO composition in an evacuated silica tube at 7003C for 2 days (6), or to reduce V O powder in a platinum crucible under an inert atmosphere at 1200}13503C for 3 days (7,8).…”