2004
DOI: 10.1016/j.jssc.2003.02.011
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Solid state phase equilibria in the Gd–Si–B system at 1270K

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Cited by 29 publications
(35 citation statements)
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“…The crystal structures of Gd 5 Si 3 and GdSi were solved from X-ray single crystal data. The structural data of the host binary phase Gd 5 Si 3 have been recently published together with those of the boron-inserted ternary Nowotny phase Gd 5 Si 3 B 0.64 [10]. The main structural results of the crystal structure of GdSi are presented in Table 1 and agree well with the ones in literature [18].…”
Section: Structural Chemistrysupporting
confidence: 78%
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“…The crystal structures of Gd 5 Si 3 and GdSi were solved from X-ray single crystal data. The structural data of the host binary phase Gd 5 Si 3 have been recently published together with those of the boron-inserted ternary Nowotny phase Gd 5 Si 3 B 0.64 [10]. The main structural results of the crystal structure of GdSi are presented in Table 1 and agree well with the ones in literature [18].…”
Section: Structural Chemistrysupporting
confidence: 78%
“…The sample package for such analysis experiments was previously reported [10]. Another part of each sample was pulverized and analyzed by X-ray diffraction (XRD) using a powder diffractometer (CPS 120 INEL) equipped with a positionsensitive detector ranging 6-120 • in 2θ.…”
Section: Methodsmentioning
confidence: 99%
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“…Finally, to reach thermodynamic equilibrium, the samples were sealed in evacuated silica tubes, heat treated at 1270 K for one month and subsequently quenched in cold water. Single crystals of Gd 5 Si 2 B 8 , resulting from a peritectic reaction between GdB 4 and Gd 5 Si 3 , [7] were obtained by crushing the solidified samples. Energy dispersive spectroscopy (EDS) and wavelength dispersive spectroscopy (WDS) using scanning electron microscopy (Jeol JSM-6400), and electron microprobe analysis (Camebax SX 50) confirmed gadolinium, silicon, and boron as the only components in the samples.…”
Section: Methodsmentioning
confidence: 99%
“…[6] Herein we describe Gd 5 Si 2 B 8 , a novel boron-rich rareearth-metal silicide boride, which has been obtained from the peritectic reaction between the binary boride GdB 4 and silicide Gd 5 Si 3 . Indeed, the solid-state phase diagram of the ternary Gd-Si-B system established at 1270 K, [7] shows a thermodynamic equilibrium between Gd 5 Si 2 B 8 and the two binary compounds GdB 4 and Gd 5 Si 3 . In addition, numerous tie lines connect Gd 5 Si 2 B 8 to the other binary phases Gd 2 B 5 , Gd 5 Si 4 , and GdSi.…”
mentioning
confidence: 99%