2019
DOI: 10.1016/j.molliq.2018.09.114
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Solubility measurement and correlation for 1-naphthoic acid in nine pure and binary mixed solvents from T = (293.15 to 333.15) K

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Cited by 25 publications
(8 citation statements)
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“…In this paper, the static equilibrium method is used for the determination. The analysis method used for the saturated supernatant is the gravimetric method to measure the solubility of 4-biphenylcarboxylic acid in nine pure solvents and methanol– n -butanol binary mixed solvents. The specific operation is as follows:…”
Section: Experimental Sectionmentioning
confidence: 99%
“…In this paper, the static equilibrium method is used for the determination. The analysis method used for the saturated supernatant is the gravimetric method to measure the solubility of 4-biphenylcarboxylic acid in nine pure solvents and methanol– n -butanol binary mixed solvents. The specific operation is as follows:…”
Section: Experimental Sectionmentioning
confidence: 99%
“…In the solid form, its extreme nitrogen atom has hydrazine moiety in the sp 3 hybridized state and the extra non-hydrogen atoms are in the sp 2 hybridized state. 5,6 Further, 1-naphthoic acid (1-naphthalene carboxylic acid) and its derivatives have attracted great attention from researchers because they possess an extensive range of biological and chemical applications in medicine, photochemicals, organic pigments, pesticides, photosensitive materials, dyes, cosmetic preparations, etc. Complexes of naphthalene derivatives have been examined since the 1960s, when 1-naphthoic acid was compiled from a planar dimer unit.…”
Section: Introductionmentioning
confidence: 99%
“…In the solid form, its extreme nitrogen atom has hydrazine moiety in the sp 3 hybridized state and the extra non-hydrogen atoms are in the sp 2 hybridized state. 5,6…”
Section: Introductionmentioning
confidence: 99%
“…Solution crystallization has a very important influence on the purity and crystallization quality of substances and is a purification method with simple operation, good effect, and wide application. 15,16 The solubility data of substances are usually used to represent the solid−liquid equilibrium data, which is the data basis for solution crystallization and plays an important role in the study of the purification process. 17,18 Therefore, in order to better guide the process of purifying DCDNB by solution crystallization, it is necessary to study its solubility in different solvents.…”
Section: Introductionmentioning
confidence: 99%
“…The synthesis of DCDNB can be divided into a one-step method or a two-step method, which can take m-dichlorobenzene and a nitrating agent as starting materials, and a mixture of nitric acid and sulfuric acid or a mixture of nitrate and sulfuric acid as the nitrating agent. Since more by-products are generated in this process, the content of DCDNB in the product is relatively low, so it is very necessary to purify. Solution crystallization has a very important influence on the purity and crystallization quality of substances and is a purification method with simple operation, good effect, and wide application. , The solubility data of substances are usually used to represent the solid–liquid equilibrium data, which is the data basis for solution crystallization and plays an important role in the study of the purification process. , Therefore, in order to better guide the process of purifying DCDNB by solution crystallization, it is necessary to study its solubility in different solvents . However, the solubility of DCDNB has not been reported in the previous literature.…”
Section: Introductionmentioning
confidence: 99%