2009
DOI: 10.2320/matertrans.mra2008177
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Spark Plasma Sintering of Mg-Based Amorphous Ball-Milled Powders

Abstract: In the present study, we report the formation of the Mg-based bulk metallic glass (BMG) samples by spark plasma sintering of the amorphous powders prepared by ball-milling. The sintering was performed in the supercooled liquid region (T g À T x ) and fully glassy Mg-based samples were successfully sintered at 398 K. The deformation on the surface associated with Vickers indentation hardness tests of the compacts reveals the presence of the semi-circular shear-bands around the indents and also reveals inhomogen… Show more

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Cited by 15 publications
(5 citation statements)
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References 21 publications
(22 reference statements)
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“…Méar et al [190] investigated Mg-based BMGs by ball milling Mg 55 Cu 30 Gd 15 and Mg 55 Cu 30 Y 15 (at.-%) gas atomised powders, for 18 and 30 h, respectively, to produce amorphous powder precursors for FAST. Fully glassy samples were successfully sintered at 125°C and Vickers hardness indents produced inhomogeneous plastic deformation.…”
Section: Sintering Of Structural Metallic Systemsmentioning
confidence: 99%
“…Méar et al [190] investigated Mg-based BMGs by ball milling Mg 55 Cu 30 Gd 15 and Mg 55 Cu 30 Y 15 (at.-%) gas atomised powders, for 18 and 30 h, respectively, to produce amorphous powder precursors for FAST. Fully glassy samples were successfully sintered at 125°C and Vickers hardness indents produced inhomogeneous plastic deformation.…”
Section: Sintering Of Structural Metallic Systemsmentioning
confidence: 99%
“…This opens up the possibility of preparing truly bulk samples through powder consolidation in supercooled liquid region. In the Zr-, Cu-, Fe-and Ni-based alloy systems, some successful consolidation of amorphous powders with wide supercooled liquid region has been achieved by warm extrusion, spark plasma sintering and equal channel angular pressing (ECAP) (Choi et al, 2007;Ishihará et al, 2002;Itoi et al, 2001;Karaman et al, 2004;Kawamura et al, 1997;Kim et al, 2009;Lee et al, 2003;Mear et al, 2009;Robertson et al, 2003;Senkov et al, 2004;Senkov et al, 2005;Sordelet et al, 2002;Zhang et al, 2006b;Zhang, et al, 2007a). The consolidated samples show almost the same thermal properties, mechanical properties, and/or soft magnetic properties as those of the BMGs prepared by direct melt casting from molted The data of the onset temperature of crystallization (T x ) and the glass transition temperature (T g ) at the heating rate of 0.67 K s -1 are also shown.…”
Section: Bulk Amorphous Alloy Consolidated From Amorphous Powder Prec...mentioning
confidence: 99%
“…For this purpose, BMGs have recently attracted much attention for biomedical applications. BMGs such as Ti-based [1][2][3], Zr-based [4], Mg-based [5,6], and Ca-based [7] are popular in the biomedical field. Ti-based and Zr-based BMGs are almost impervious to corrosion in the human body; hence they are suitable for permanent implant.…”
Section: Introductionmentioning
confidence: 99%
“…And Mg-based and Ca-based BMGs for temporary due to be easily corroded by body fluids [5,7]. Compared to other materials, Mg is exceptionally light in weight with a density of around 1.74 g/cm 3 , and the elastic modulus of Mg is similar to that of natural bone [6]. Further, the ability for magnesium alloys to undergo biodegradation eliminates the requirement for a second surgery to remove the implant.…”
Section: Introductionmentioning
confidence: 99%