2018
DOI: 10.1002/celc.201800578
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Spectro‐Electrochemical Microfluidic Platform for Monitoring Multi‐Step Cascade Reactions

Abstract: Benefits of utilizing cascade reactions for chemical synthesis include minimizing waste and decreasing experimentation times. However, these complex systems lack an efficient screening platform for evaluating their progression. A paper‐based microfluidic platform was developed to monitor cascade systems without the need for off‐line product verification. Two types of paper‐based platforms were fabricated to facilitate this study: electrochemical and spectro‐electrochemical. Electrochemical platforms were integ… Show more

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Cited by 10 publications
(16 citation statements)
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“…[24] In the present work, the full oxidation of glycerol to CO 2 was chosen to illustrate the concept of using multiple modalities of catalysts in series on 3D platforms. [24] In the present work, the full oxidation of glycerol to CO 2 was chosen to illustrate the concept of using multiple modalities of catalysts in series on 3D platforms.…”
Section: Resultsmentioning
confidence: 99%
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“…[24] In the present work, the full oxidation of glycerol to CO 2 was chosen to illustrate the concept of using multiple modalities of catalysts in series on 3D platforms. [24] In the present work, the full oxidation of glycerol to CO 2 was chosen to illustrate the concept of using multiple modalities of catalysts in series on 3D platforms.…”
Section: Resultsmentioning
confidence: 99%
“…Molecular catalysts are oxidation catalyst capable of oxidizing alcohols and aldehydes. [24] The oxidation of glycerol, glyceraldehyde, glyceric acid, tartronic acid, and glyoxylic acid was performed with the pyreneÀ amidoÀ TEMPO on a 2D electrochemical platform to verify catalytic activity ( Figures S1-2, SI). [25] TEMPO is a stable nitroxyl radical; modification of its native form with an NH 2 group enhances the electrocatalytic activity 8x at pH = 5.2 with a 70 % conversion rate of glycerol.…”
Section: Resultsmentioning
confidence: 99%
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