“…Above this composition (x = 0.15) the a parameter remain practically constant and impurity phases identified to both tetragonal and monoclinic ZrO 2 starts to appear. It is known that ZrO 2 has three polymorphs: monoclinic (m-phase, below 1170 °C), tetragonal (t-phase, between 1170 and 2370 °C) and cubic (cphase, above 2370 °C) [19,20]. In order to check the reproducibility of the synthesis procedure, two sets of samples were prepared, using the same preparative method, namely 1 st and 2 nd preparation, respectively.…”