Looking back to the four years and three months that my Ph.D. journey took at IMDEA Materials Institute and the Polytechnic University of Madrid, I wish to express my sincerest and deepest gratitude to many people who offered me their support and help since the first day I arrived at IMDEA. First of all, I would like to express my most sincere gratitude to my supervisor Dr. Jon Molina. We did not even have a Skype meeting before and we only met after two months since I arrived at IMDEA. Thanks for your trust, for providing me with the opportunity to work in your group and for guiding me fully and patiently along this journey. At the beginning, I was new to the nanomechanical field, but you explained patiently the fundamental theory to me and checked the work carefully during each meeting. Gradually, you gave me a lot of freedom and your passion encouraged me to get deeper and deeper into the field. You helped me overcoming the difficulties and avoiding the mistakes that we often make when we work in a quick, eager and impetuous way, without deeper thinking. I still remember one day clearly, when you made me realize how natural aging at room temperature could influence the results on supersaturated Mg-Zn solid solutions. This made us introduce the topic of Zn distribution by studying the diffusion couple in the as-quenched, room aged and peak aged conditions. I also want to thank you for teaching me to think in a critical way, to improve my scientific writing and to help me differentiate between experimental evidence and mere speculation. Many thanks for all your wisdom guidance and continuous encouragement to help me grow during my study and work at IMDEA. Without your scholarly inputs and valuable guidance, this thesis would have not been possible. Your passion and solid background in materials science inspire me to continue working on materials research in the future. I feel so grateful and fortunate for having been working under your supervision and for growing up in our pleasant and exciting group. I also own my most sincere thanks to my other supervisor, Dr. Yuwen Cui, with whom I worked since I joined IMDEA Materials. Despite your departure one year later to Nanjing Tech University, you have remained deeply involved in my thesis. Your guidance, great patience and insightful vision was essential to introduce me in the field of high-throughput development of Mg alloys. I also wish to thank IMDEA Materials Institute for offering me such a fantastic environment for scientific research. I'm grateful for the financial support from the China Scholarship Council. My special thanks go to my colleagues: Dr. Miguel Monclus, thanks for your assistance with performing nanomechanical tests, which were always very timeconsuming; and Dr. Miguel Castillo, thanks for your help with the TEM characterizations and for training in the FIB. Special thanks to Dr. Lingwei Yang and Dr. Chuanyun Wang. You two taught and helped me a lot in micropillar testing and TEM lamellar preparation and also helped me analyse the data even during...