Abstractwere prepared by solid state reaction method. The crystal structure, microstructure, and magnetic properties were characterized using powder X-ray diffraction, scanning electron microscope (SEM) and permagraph meter, respectively. The results show that the nanocrystalline BaFe 12−2 Co Ti O 19 has single phase with polycrystalline structure, the grain size decrease by doping, the coercivity (Hc) and saturation magnetization (Ms) decrease with increasing Co-Ti substitutions.