Monodisperse zinc oxide (ZnO) nanoparticles were synthesized using ultrasonically atomized precursor mist in simple
chemical route at low temperature. Analytical grade sodium hydroxide and zinc chloride were dissolved in 100 ml
methanol. Zinc chloride precursor solution was converted into very fine mist (atomized) using a nozzle (Sono-Tek
Corporation, U.S.A.) operated at ultrasonic frequency of 120 KHz. Fine mist droplets were added slowly (50ml/
hour) into sodium hydroxide solution in 2 hours. The NaOH solution in beaker turned slowly into white product due
to addition of zinc chloride. The white product was kept in constant temperature bath at 90°C for 3 hours. The white
product was washed five times using double distill water and dried in oven for 2 hours. Different powder samples were
synthesized using same procedure by changing the molarity of sodium hydroxide keeping the molarity of zinc chloride
and other preparative conditions same. The structural, microstructural, thermal and optical properties of fine powders
were analyzed using X Ray Diffractometer, Scanning Electron Microscopy, Simultaneous Thermal Analyzer, UV-Vis
Spectroscopy and Photoluminescence Spectroscopy. Fine ZnO nanorods, elongated and spherical nanoparticles were
observed due to change in molarity of NaOH. The results are discussed and interpreted.