Surface Metal Complexes and Their Applications

Kistler, Joseph D.; Serna, Pedro; Asakura, Kiyotaka; Gates, Bruce C.

doi:10.1002/9781118844243.ch26

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An Approach For Synthesis Of Supported Mononuclear Metal Com...1

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Cited by 2 publications

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“…Some good books and articles regarding detailed XAFS analysis have been reported with theory and illustrative examples [13,14]. Kistler et al [40] reported an example of detailed analysis procedures about how candidate structural models are constructed and examined, and a recommended structural model is obtained.…”

Section: An Approach For Synthesis Of Supported Mononuclear Metal Com...mentioning

confidence: 99%

X-ray absorption spectroscopy for single-atom catalysts: Critical importance and persistent challenges

Ogino

2017

Chinese Journal of Catalysis

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Section: An Approach For Synthesis Of Supported Mononuclear Metal Com...mentioning

confidence: 99%

X-ray absorption spectroscopy for single-atom catalysts: Critical importance and persistent challenges

Ogino

2017

Chinese Journal of Catalysis

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Development of Surface Fluorescence X‐Ray Absorption Fine Structure Spectroscopy Using a Laue‐Type Monochromator

Wakisaka

Kido

Uehara

et al. 2018

The Chemical Record

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Surface fluorescence X-ray absorption fine structure (XAFS) spectroscopy using a Laue-type monochromator has been developed to acquire structural information about metals with a very low concentrate on a flat highly oriented pyrolytic graphite (HOPG) surface in the presence of electrolytes. Generally, surface fluorescence XAFS spectroscopy is hindered by strong scattering from the bulk, which often chokes the pulse counting detector. In this work, we show that a bent crystal Laue analyzer (BCLA) can efficiently remove the scattered X-rays from the bulk even in the presence of solution. We applied the technique to submonolayer (∼10 atoms cm ) Pt on HOPG and successfully obtained high signal/noise in situ XAFS data in combination with back-illuminated fluorescence XAFS (BI-FXAFS) spectroscopy. This technique allows in situ XAFS measurements of flat electrode surfaces to be performed in the presence of electrolytes.

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Surface Metal Complexes and Their Applications

Cited by 2 publications

References 74 publications

X-ray absorption spectroscopy for single-atom catalysts: Critical importance and persistent challenges

X-ray absorption spectroscopy for single-atom catalysts: Critical importance and persistent challenges

Development of Surface Fluorescence X‐Ray Absorption Fine Structure Spectroscopy Using a Laue‐Type Monochromator

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