Sustainable electrocatalytic oxidation of <i>N</i>-alkylamides to acyclic imides using H<sub>2</sub>O

Qi, Jing; Wang, Xiyan; Wang, Gan; Dubbaka, Srinivas Reddy; O'Neill, Patrick; Ang, Hwee Ting; Wu, Jie

doi:10.1039/d3gc04010k

Green Chem.

2024

DOI: 10.1039/d3gc04010k

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Sustainable electrocatalytic oxidation of N-alkylamides to acyclic imides using H₂O

Jing Qi,

Xiyan Wang,

Gan Wang

et al.

Abstract: Green and environmentally friendly synthesis of imides from N-alkylamides via electrocatalytic oxidation with H2O as the oxygen source, yielding versatile imide building blocks for biologically relevant 1,2,4-triazole compounds.

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Electrochemical C−H Hydroxylation and Alkoxylation Reactions

Wang,

Zhang,

2024

ChemSusChem

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The electrochemical C‐H hydroxylation and alkoxylation reactions have emerged as sustainable platforms to construct valuable oxygenated compounds such as alcohols, phenols, and ethers. Compared with traditional approaches, these electrochemical strategies not only enhance the atom economy through bypassing the use of chemical oxidants but also unlock new reactivities by accessing reactive intermediates under mild conditions. In this review, we tried to provide an overview of the representative achievements in this field since 2020. The related transformations are classified into five parts according to the underlying mechanisms. Furthermore, the potential opportunities and challenges within this rapidly emerging field were also discussed. This review is not intended to be exhaustive but rather to illustrate the synthetic potential of electrochemical C‐H hydroxylation and alkoxylation strategies in the sustainable and selective assembly of valuable oxygenated compounds.

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Electrochemical C−H Hydroxylation and Alkoxylation Reactions

Wang,

Zhang,

2024

ChemSusChem

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DMAP-promoted oxidative functionalization of α-amino ketones via oxygen delivery from water/alcohols

Wang,

Liu,

Zheng

et al. 2024

Chem. Commun.

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Sustainable electrocatalytic oxidation of N-alkylamides to acyclic imides using H₂O

Abstract: Green and environmentally friendly synthesis of imides from N-alkylamides via electrocatalytic oxidation with H2O as the oxygen source, yielding versatile imide building blocks for biologically relevant 1,2,4-triazole compounds.

Cited by 2 publications

References 31 publications

Electrochemical C−H Hydroxylation and Alkoxylation Reactions

Electrochemical C−H Hydroxylation and Alkoxylation Reactions

DMAP-promoted oxidative functionalization of α-amino ketones via oxygen delivery from water/alcohols

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Sustainable electrocatalytic oxidation of N-alkylamides to acyclic imides using H2O

Abstract: Green and environmentally friendly synthesis of imides from N-alkylamides via electrocatalytic oxidation with H2O as the oxygen source, yielding versatile imide building blocks for biologically relevant 1,2,4-triazole compounds.

Cited by 2 publications

References 31 publications

Electrochemical C−H Hydroxylation and Alkoxylation Reactions

Electrochemical C−H Hydroxylation and Alkoxylation Reactions

DMAP-promoted oxidative functionalization of α-amino ketones via oxygen delivery from water/alcohols

Contact Info

Product

Resources

About

Sustainable electrocatalytic oxidation of N-alkylamides to acyclic imides using H₂O