1975
DOI: 10.1016/s0040-4039(00)71903-4
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Synthese de p-methyl et p-phenyl spirophosphoranes a partir de diols ou d'aminoalcools

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Cited by 15 publications
(4 citation statements)
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“…Other reagents were used as received. Cp(CO) 2 RuCl, HP(OC 6 H 4 NH) 2 , and o -C 6 H 4 (NHMe)(OH) were prepared according to the respective published procedures.…”
Section: Methodsmentioning
confidence: 99%
“…Other reagents were used as received. Cp(CO) 2 RuCl, HP(OC 6 H 4 NH) 2 , and o -C 6 H 4 (NHMe)(OH) were prepared according to the respective published procedures.…”
Section: Methodsmentioning
confidence: 99%
“…Essentially two methods have been applied to introduce alkoxy substituents on a phosphorus atom: the alcoholysis of aminophosphine derivatives [6][7][8][9][10] or the reaction of chlorophosphine derivatives with an alcohol in the presence of a tertiary amine base [11][12][13][14][15]. Triphosphine ligands of the type RP[CH 2 CH 2 CH 2 P(OR) 2 ] 2 have not been reported previously.…”
Section: Preparation Of the Tridentate Phosphine Ligands I-ivmentioning
confidence: 99%
“…for C 18 12.2.8. Fe(CyP[CH 2 CH 2 CH 2 P(OMe) 2 ] 2 )(CO) 2 (8) The phosphine ligand IV (1 g, 2.6 mmol) and Fe(CO) 5 (0.35 mL, 2.6 mmol) in 25 mL of benzene were irradiated from the outside for 5 h at room temperature with constant stirring. The benzene was removed under vacuum and the residue was purified by column chromatography (benzene/THF).…”
Section: General Procedures To Obtain I-ivmentioning
confidence: 99%
“…Similarly, the reactions of tricoordinated organophosphorus precursors 129-131 with an appropriate equivalent of ethylene glycol was found to give the spirophosphorane 132. All the three reactions occurred via the bis-ester 133 formed in a nucleophilic exchange reaction at the tricoordinated phosphorus center of precursors 129-131 [108] (Scheme 54). …”
Section: P-1c-4o Phosphoranesmentioning
confidence: 99%