2011
DOI: 10.4236/wjcmp.2011.12008
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Synthesis and Characterization of Superparamagnetic Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub> Core-Shell Composite Nanoparticles

Abstract: The Fe 3 O 4 @SiO 2 composite nanoparticles were obtained from as-synthesized magnetite (Fe 3 O 4) nanoparticles through the modified Stöber method. Then, the Fe 3 O 4 nanoparticles and Fe 3 O 4 @SiO 2 composite nanoparticles were characterized by means of X-ray diffraction (XRD), Raman spectra, scanning electron microscope (SEM) and vibrating sample magnetometer (VSM). Recently, the studies focus on how to improve the dispersion of composite particle and achieve good magnetic performance. Hence effects of the… Show more

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Cited by 89 publications
(30 citation statements)
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“…[58] Figure 2C shows the high-resolution spectra for O 1s in Fe 3 O 4 @pDA and Fe 3 O 4 @pDA150, in which a clear shift to lower binding energies is also observed after thermal treatment. [58] Figure 2C shows the high-resolution spectra for O 1s in Fe 3 O 4 @pDA and Fe 3 O 4 @pDA150, in which a clear shift to lower binding energies is also observed after thermal treatment.…”
Section: Xpsmentioning
confidence: 99%
“…[58] Figure 2C shows the high-resolution spectra for O 1s in Fe 3 O 4 @pDA and Fe 3 O 4 @pDA150, in which a clear shift to lower binding energies is also observed after thermal treatment. [58] Figure 2C shows the high-resolution spectra for O 1s in Fe 3 O 4 @pDA and Fe 3 O 4 @pDA150, in which a clear shift to lower binding energies is also observed after thermal treatment.…”
Section: Xpsmentioning
confidence: 99%
“…The reaction between an alkoxysilane and a solid material does not involve a single mechanism, and many different intermediates are possible [15,16].…”
Section: Aptes Coating Mechanism On Fe 3 O 4 Magnetite Nanoparticlesmentioning
confidence: 99%
“…However, during the baking before the composite starts crosslinking, the SPMPC reflows although the samples are brought directly to 160 °C with no ramp. As a first consequence, a fraction of the particle alignment is lost but no influence on the Fe 3 O 4 NP properties is expected [30]. This particle alignment reduction is revealed by the slight blurring of the lines visible in Figure 6a showing the same microstructure before (Figure 6a upper image) and after curing (Figure 6a lower image).…”
Section: Induced Preferential Magnetic Directionsmentioning
confidence: 88%