2007
DOI: 10.1002/chin.200716119
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Synthesis of 2‐Alkyl‐Substituted Benzimidazoles by Thermal Decomposition of 2‐Azidobenzenamines in the Presence of an Aldehyde.

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“…Literature provided the precedent of diazotization reaction followed by nucleophilic displacement by sodium azide 33,34. This approach was used to synthesize 5-azidonicotinic acid 3i starting from 5-aminonicotinic acid 3a (Scheme 5).…”
Section: Chemistrymentioning
confidence: 99%
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“…Literature provided the precedent of diazotization reaction followed by nucleophilic displacement by sodium azide 33,34. This approach was used to synthesize 5-azidonicotinic acid 3i starting from 5-aminonicotinic acid 3a (Scheme 5).…”
Section: Chemistrymentioning
confidence: 99%
“…32 Literature provided the precedent of diazotization reaction, followed by nucleophilic displacement by sodium azide. 33,34 This approach was used to synthesize 5-azidonicotinic acid 3i starting from 5-aminonicotinic acid 3a (Scheme 5). We started with protection of the acid group in 5-aminonicotinic acid (3a) with a hydrophobic ethyl ester (10), followed by conversion of the amine into an azide using diazotization chemistry to give 11.…”
Section: Chemistrymentioning
confidence: 99%
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