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This study explores the controlled, continuous production of thin carbon rods between graphite electrodes (continued electrode deposits) during an arc discharge of high voltage alternating current with a frequency of 50 Hz in liquid paraffin, along with in situ doping of the resulting material using a suspension of liquid paraffin and iron powder ( <10 μm). The surface morphology of the obtained carbon rod nanomaterials was characterized using scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDX), scanning transmission electron microscopy (STEM) with EDX chemical composition analysis, X-ray microtomography (micro-CT), and atomic force microscopy (AFM). The AFM technique in scanning thermal microscopy (SThM) and conductive probe (CP) modes was employed to determine the temperature and electrical conductivity of the obtained nanostructures. Qualitative analysis was conducted using Raman spectroscopy, X-ray powder diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). This simple system for producing thin, stable carbon wires (< 1.2 mm thick) enables efficient and low-cost production and doping of these materials. The high-voltage alternating current (HVAC) arc discharge method for growing controlled, metal-doped electrode deposits presents a new approach to producing inexpensive, porous carbon nanomaterials for various scientific and technological applications.
This study explores the controlled, continuous production of thin carbon rods between graphite electrodes (continued electrode deposits) during an arc discharge of high voltage alternating current with a frequency of 50 Hz in liquid paraffin, along with in situ doping of the resulting material using a suspension of liquid paraffin and iron powder ( <10 μm). The surface morphology of the obtained carbon rod nanomaterials was characterized using scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDX), scanning transmission electron microscopy (STEM) with EDX chemical composition analysis, X-ray microtomography (micro-CT), and atomic force microscopy (AFM). The AFM technique in scanning thermal microscopy (SThM) and conductive probe (CP) modes was employed to determine the temperature and electrical conductivity of the obtained nanostructures. Qualitative analysis was conducted using Raman spectroscopy, X-ray powder diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). This simple system for producing thin, stable carbon wires (< 1.2 mm thick) enables efficient and low-cost production and doping of these materials. The high-voltage alternating current (HVAC) arc discharge method for growing controlled, metal-doped electrode deposits presents a new approach to producing inexpensive, porous carbon nanomaterials for various scientific and technological applications.
Heavy metal contamination in water sources poses a significant threat to environmental and public health, necessitating effective remediation strategies. Nanomaterial-based approaches have emerged as promising solutions for heavy metal removal, offering enhanced selectivity, efficiency, and sustainability compared to traditional methods. This comprehensive review explores novel nanomaterial-based approaches for heavy metal remediation, focusing on factors such as selectivity, regeneration, scalability, and practical considerations. A systematic literature search was conducted using multiple academic databases, including PubMed, Web of Science, and Scopus, to identify relevant articles published between 2013 and 2024. The review identifies several promising nanomaterials, such as graphene oxide, carbon nanotubes, and metal-organic frameworks, which exhibit high surface areas, tunable surface chemistries, and excellent adsorption capacities. Surface functionalization with specific functional groups (e.g., carboxyl, amino, thiol) significantly enhances the selectivity for target heavy metal ions. Advances in regeneration strategies, including chemical desorption, electrochemical regeneration, and photocatalytic regeneration, have improved the reusability and cost-effectiveness of these materials. Scalability remains a critical challenge, but recent developments in synthesis methods, such as green synthesis and continuous-flow synthesis, offer promising solutions for large-scale production. The stability and longevity of nanomaterials have been improved through surface modification and the development of hybrid nanocomposites. Integrating nanomaterials with existing water treatment infrastructure and combining them with other remediation techniques, such as membrane filtration and electrochemical methods, can enhance overall treatment efficiency and feasibility. In conclusion, nanomaterial-based approaches hold immense promise for revolutionizing heavy metal remediation and advancing sustainable water management practices. As future research is geared towards retrofitting existing treatment plants, it is equally critical to mitigate unintended environmental and public health consequences associated with the widespread production and use of nanomaterials, such as their leachability into water systems and environmental persistence.
Carbonaceous materials have gained significant attention in recent years for their various applications in the field of medicine and biotechnology. This comprehensive review explores the synthesis and characterization of carbon-based materials and their potentials in various medical applications. The paper delves into the methods of fabrication of carbon-based nanoparticles, such as carbon nanotubes, biochar, and graphene, while highlighting their unique properties. Characterization techniques, such as microscopy, spectroscopy, and surface analysis, are discussed to provide insights into the chemical and structural properties of these materials. Furthermore, the review examined their wide-ranging medical applications, encompassing tissue engineering, drug delivery, biosensing, and imaging, showcasing the versatility and promising contributions of carbonaceous materials in the healthcare industry. The review outlines the current challenges and prospects in the field, emphasizing the growing significance of carbon-based materials as valuable tools in advancing medical science and technology, as well as public health.
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