2013
DOI: 10.1016/j.molstruc.2013.05.008
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Synthesis, stereochemical, structural and biological studies of some 2,6-diarylpiperidin-4-one N(4′)-cyclohexyl thiosemicarbazones

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Cited by 20 publications
(9 citation statements)
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“…The compounds HL and (1) were solubilized in CDCl 3 , while complex (2) was solubilized in DMSO-d 6 due to their better solubility in these deuterated solvents. The presence of multiplets in opposite displacements referring to the terminal rings in thiosemicarbazone is observed in HL [30][31][32]. The cyclohexyl-thiosemicarbazone molecule is reported with their respective protons represented as two close multiplets that can be identified in their equatorial and axial form.…”
Section: Spectroscopy Analysismentioning
confidence: 88%
“…The compounds HL and (1) were solubilized in CDCl 3 , while complex (2) was solubilized in DMSO-d 6 due to their better solubility in these deuterated solvents. The presence of multiplets in opposite displacements referring to the terminal rings in thiosemicarbazone is observed in HL [30][31][32]. The cyclohexyl-thiosemicarbazone molecule is reported with their respective protons represented as two close multiplets that can be identified in their equatorial and axial form.…”
Section: Spectroscopy Analysismentioning
confidence: 88%
“…The ligand 13 C-NMR spectra (Figure 4) showed a signal at 178.42, 174.93 ppm which could be assigned to the carbon atoms of thioketone (C 15 = S), [56,57] and carbonyl carbon of khellin moiety (C 11 = O), [57,58] respectively. …”
Section: C-nmr Spectramentioning
confidence: 99%
“…Thiosemicarbazone is emerging moiety with a wide spectrum of biological activity and having sound scope in research and developing process in pharmaceutical and medicinal chemistry . Thiosemicarbazones are of considerable interest because of their chemistry and potentially beneficial biological activity, such as antibacterial , antifungal , antiviral , ant‐amoebic , antimalarial, and antitumor activity . Thiosemicarbazones are also used as ligands in the field of inorganic chemistry for the formation of metal complexes due to the presence of thionic sulfur and the azomethine nitrogen .…”
Section: Introductionmentioning
confidence: 99%
“…Thiosemicarbazones are of considerable interest because of their chemistry and potentially beneficial biological activity, such as antibacterial [9], antifungal [10], antiviral [11], ant-amoebic [12], antimalarial, and antitumor activity [13]. Thiosemicarbazones are also used as ligands in the field of inorganic chemistry for the formation of metal complexes due to the presence of thionic sulfur and the azomethine nitrogen [14].…”
Section: Introductionmentioning
confidence: 99%