Highly resistive molecular beam epitaxial GaN layers are characterized by temperature dependent conductivity and Hall effect measurements. Seven n-type GaN samples with room temperature layer resistivity ranging between 8 and 4.2ϫ10 6 ⍀ cm are used in this study. The experimental data are analyzed by considering various transport models such as band and hopping conduction, scattering on charged dislocations and grain boundaries controlled transport. The same defect level of 0.23 eV, attributed to nitrogen vacancy, is found for layers with 300 р3.7ϫ10 3 ⍀ cm. The Hall mobility for two lower resistivity layers is influenced mainly by phonon scattering (H ϳT x , xϭϪ1.4). However, higher resistivity layers show positive mobility power, xϭ0.5-0.9, which can be explained by dominating scattering on charged dislocations. Properties of layers with the highest resistivity ͑1ϫ10 5 and 4.2ϫ10 6 ⍀ cm͒ and extremely low Hall mobility ͑6 and Ͻ0.1 cm 2 V Ϫ1 s Ϫ1 ͒ are consistent with grain boundary controlled transport. The barrier height between grains of 0.11 eV and an average grain size of 200 nm are found. Neither nearest-neighbor or variable range single phonon hopping nor multiphonon hopping can be clearly attributed to the conduction of the layers investigated.