“…† As observed, CP calcined at 400-600 C for 1-4 h presented peaks at wavenumbers of 3500 cm À1 (-OH and -NH), 2900 cm À1 (C-H), 1735 cm À1 , 1600 cm À1 (C]O and C]C), 1217 cm À1 , 1114 cm À1 and 1030 cm À1 (C-O), which should be attributed to the vibrations of various acidbase functional groups, such as carboxylic, lactone, phenolic and amino groups. 17 Here, the calcination temperature and time had signicant effects on the enhancement of carbonyl group levels. However, the decomposition of these functional groups on activated CP may occurred with conversion into CO 2 in the case of excessively high calcination temperatures and long calcination times being applied, leading to deactivation and the low performance of the adsorbent for metal cation removal.…”