Single‐, two‐, and three‐stage homogenization treatments of heat‐resistant alloy 2618 were conducted in this study. Results reveal a low melting point Al2CuMg phase and high melting point Al2Cu phase in the as‐cast aluminum alloy 2618. After single‐stage homogenization at 495 °C for 10 h, the Al2CuMg phase dissolves completely, but the Al2Cu phase cannot be completely dissolved even once the homogenization time is prolonged to 18 h. After the alloy 2618 are homogenized using two stages: 495 °C for 10 h and 520 °C for 8 h, a portion of the Al2Cu phase remains in the alloy. The Al2Cu phase remains undissolved even after prolonged time. After the two‐stage homogenization treatment at 495 °C for 10 h and 540 °C for 5 h, the high melting point Al2Cu phase completely dissolves but overburn occurs. After the alloy 2618 are homogenized using three stages at 495 °C for 10 h, 520 °C for 5 h, and 540 °C for 3 h, the Al2Cu phase completely dissolves and no overburn is detected. The three‐stage homogenization treatment is an effective method for dissolving the high melting point Al2Cu phase in the alloy 2618 and increasing their overburn temperature and solid solution temperature.