1934
DOI: 10.1021/ja01324a032
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The Preparation of l-Abietic Acid (Schulz) and Properties of Some of its Salts1

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Cited by 23 publications
(10 citation statements)
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“…Abietic acid was isolated from crude abietic acid (Aldrich, 70%) using dipentylamine. 10 Tetramethylammoniumbromide (TMAB) (Aldrich, 98%) was used as received. 2,2'-Azobisisobutyronitrile (AIBN) of reagent grade was recrystallized from methanol.…”
Section: Methodsmentioning
confidence: 99%
“…Abietic acid was isolated from crude abietic acid (Aldrich, 70%) using dipentylamine. 10 Tetramethylammoniumbromide (TMAB) (Aldrich, 98%) was used as received. 2,2'-Azobisisobutyronitrile (AIBN) of reagent grade was recrystallized from methanol.…”
Section: Methodsmentioning
confidence: 99%
“…Abietic acid was isolated from crude abietic acid (Aldrich, 70%) using dipentylamine. 7 The melting point was 167-169 • C. 2, 2 -Azobisisobutyronitrile (AIBN) of reagent grade was recrystallized from methanol. Methyl methacrylate (MMA) of reagent grade was distilled in the presence of hydroquinone under reduced pressure.…”
Section: Methodsmentioning
confidence: 99%
“…通过运用硅胶、Sephadex LH-20 凝胶和半制备型 HPLC 等色谱分离纯化手段, 从大别山五针松(P. dabeshanensis)松针(干重 30 g)的 90%甲醇提取物中共分离得 到 10 个二萜类化合物(图 1). 通过对比文献以及分析其 理化数据, 其中 9 个已知二萜化合物分别被鉴定为 7callitrisic acid (2) [7] 、abieta-7,13-diene-18-oic acid (3) [7~9] 、 isopimara-7-en-18-oic acid (4) [10,11] 、8 14-podocarpen-13on-18-oic acid (5) [12] 、trans-abienol (6) [13] 、3β-hydroxy-12,13E-biformen (7) [14] 、lambertianic acid (8) [15~17] 、16ξhydroxpinusolidic acid (9) [15] 、15ξ-hydroxpinusolidic acid (10) [15] . [7] 的结构非常相似, 区别仅在于化合 [6,18] .…”
Section: 结果与讨论unclassified