The Synthesis and Co(II), Ni(II), Cu(II) and Uo<sub>2</sub>(Vi) Complexes of 1,2-O-Benzal-4-Aza-7-Aminoheptane

Şekerci, Memet; Alkan, Cihan

doi:10.1080/00945719909351728

Cited by 17 publications

(1 citation statement)

References 19 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…The IR spectra of [Cu(L 1 )(OAc) 2 ]∙5H 2 O, [Zn(L 1 )(OAc) 2 (H 2 O) 2 ]∙3H 2 O, [Cu 2 (L 2 )(OAc) 4 ]∙2H 2 O∙2DMF and [Zn 2 (L 2 )(OAc) 4 (H 2 O) 4 ]∙5H 2 O show two new bands at 1555 and 1384 cm −1 assignable to the ν as (C–O) and ν s (C–O) bands of the acetate group [23,24], respectively, which are consistent with monodentate acetate coordination. The IR spectra of the [Cu(L 1 )(NO 3 )H 2 O]∙NO 3 ∙3.5H 2 O, [Zn(L 1 )(NO 3 ) 2 ]∙4.5H 2 O and [Zn(L 2 ) 2 (NO 3 ) 2 ]∙DMF complexes show strong bands at 1385 and 1285 cm −1 assigned to ν as (NO 3 − ) and ν s (NO 3 − ), respectively, indicating the presence of terminally bounded monodentate nitrate groups [25,26].…”

Section: Resultsmentioning

confidence: 99%

Synthesis, Structural Characterization and Biological Activity of Novel Cyclohexane-1,3-dione Ligands and Their Metal Complexes

et al. 2015

View full text Add to dashboard Cite

Some new Zn(II) and Cu(II) complexes [Cu(LC-NMR and ultraviolet (UV-Vis.) spectroscopy, elemental analysis, magnetic susceptibility, mass spectrometry and thermogravimetrydifferential thermal analysis (TGA-DTA). The synthesized ligands and their complexes were tested for antibacterial activity against Escherichia coli ATCC 25922, Enterococcus faecalis ATCC 29212, Staphylococcus aureus ATCC 25923, and Salmonella typhimurium CCM 583. Some of complexes showed medium-level antibacterial activity against the test bacteria compared with ampicillin.

show abstract

Section: Resultsmentioning

confidence: 99%

Synthesis, Structural Characterization and Biological Activity of Novel Cyclohexane-1,3-dione Ligands and Their Metal Complexes

et al. 2015

View full text Add to dashboard Cite

show abstract

The synthesis and characterization of 1,2-O-cyclohexylidene-4-aza-8-aminooctane and some of its transition metal complexes

ekerci

2000

Heteroatom Chem.

View full text Add to dashboard Cite

1,2‐O‐Cyclohexylidene‐4‐aza‐8‐aminooctane (L) has been synthesized starting from 1‐chloro‐2,3‐O‐cyclohexylidene, which has been prepared by the reaction of epichlorohydrin with cyclohexanone. The complexes of this ligand with Co(II), Ni(II), Cu(II), and UO2(VI) salts were prepared. The structures of the ligand and its complexes are proposed based on elemental analyses, IR, UV‐vis, 1H, and 13C NMR spectra, magnetic susceptibility measurements, thermogravimetric analyses, and differential thermal analyses. © 2000 John Wiley & Sons, Inc. Heteroatom Chem 11:254–260, 2000

show abstract

Synthesis, characterization and thermal behavior of some Zn(II) complexes with ligands having 1,3,4‐thiadiazole moieties

Turan

Şekerci

2010

Heteroatom Chemistry

Self Cite

View full text Add to dashboard Cite

Some new zinc(II) complexes of the type [Zn(L1)2(C2H5OH)2]·C2H5OH, [Zn(L2)2 Cl2]·H2O, and [Zn2(L3)2(H2O)4Cl4], where HL1 = N‐[5′‐amino‐2, 2′‐bis(1,3,4‐thiadiazole)‐5‐yl]‐2‐hydroxybenzaldehyde imine, L2 = N‐(5‐ethyl‐1,3,4‐thiadiazole‐2‐yl)tereph‐ thalaldehyde imine, and L3 = N,N′‐bis[5‐(4‐nitro phenyl)‐1,3,4‐thiadiazole‐2‐yl]terephthalaldehydedii‐ mine have been synthesized and characterized by IR, 1H NMR spectra, elemental analyses, magnetic susceptibility, UV–vis. and thermogravimetry‐differential thermal analysis (TGA‐DTA). On the basis of electronic spectral studies, an octahedral environment around the Zn(II) ion has been suggested. 1H NMR spectra of the metal complexes of ligands were found to be in agreement with the proposed stoichiometry. The presence of water molecules and ethanol in the Zn(II) complexes is also indicated by the thermal studies. © 2010 Wiley Periodicals, Inc. Heteroatom Chem 21:14–23, 2010; Published online in Wiley InterScience (http://www.interscience.wiley.com). DOI 10.1002/hc.20572

show abstract

The Synthesis and Co(II), Ni(II), Cu(II) and Uo₂(Vi) Complexes of 1,2-O-Benzal-4-Aza-7-Aminoheptane

Abstract: 1,3,-O-BenI-4-~-7-aminohcptanc (L) has bccn synthesizcd starting from

Cited by 17 publications

References 19 publications

Synthesis, Structural Characterization and Biological Activity of Novel Cyclohexane-1,3-dione Ligands and Their Metal Complexes

Synthesis, Structural Characterization and Biological Activity of Novel Cyclohexane-1,3-dione Ligands and Their Metal Complexes

The synthesis and characterization of 1,2-O-cyclohexylidene-4-aza-8-aminooctane and some of its transition metal complexes

Synthesis, characterization and thermal behavior of some Zn(II) complexes with ligands having 1,3,4‐thiadiazole moieties

Contact Info

Product

Resources

About

The Synthesis and Co(II), Ni(II), Cu(II) and Uo2(Vi) Complexes of 1,2-O-Benzal-4-Aza-7-Aminoheptane

Abstract: 1,3,-O-Ben~~I-4-~~~-7-aminohcptanc (L) has bccn synthesizcd starting from

Cited by 17 publications

References 19 publications

Synthesis, Structural Characterization and Biological Activity of Novel Cyclohexane-1,3-dione Ligands and Their Metal Complexes

Synthesis, Structural Characterization and Biological Activity of Novel Cyclohexane-1,3-dione Ligands and Their Metal Complexes

The synthesis and characterization of 1,2-O-cyclohexylidene-4-aza-8-aminooctane and some of its transition metal complexes

Synthesis, characterization and thermal behavior of some Zn(II) complexes with ligands having 1,3,4‐thiadiazole moieties

Contact Info

Product

Resources

About

The Synthesis and Co(II), Ni(II), Cu(II) and Uo₂(Vi) Complexes of 1,2-O-Benzal-4-Aza-7-Aminoheptane

Abstract: 1,3,-O-BenI-4-~-7-aminohcptanc (L) has bccn synthesizcd starting from