Thermoluminescence of the epoxy resin Epidian‐5

Subocz, J.

doi:10.1002/actp.1986.010370503

Acta Polymerica

1986

DOI: 10.1002/actp.1986.010370503

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Thermoluminescence of the epoxy resin Epidian‐5

J. Subocz

Abstract: Aus verarbeitungstechnischer Sicht wird ein Uberblick zur rheologischen Stoffcharakterisierung, insbesondere bei Verfestigungsprozessen, gegeben, in dessen Mittelpunkt der Phasenubergang flussig-fest steht.

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1988

1989

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Effects of thermal ageing on thermoluminescence of an epoxy resin composition

Subocz

1989

Acta Polymerica

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Thermal ageing of Epidian-2 epoxy resin results in quenching and decrease in energetic depth of dopant thermoluminescence (TL) centres. The existing correlation between the depths or TL centres and the contents of methylene and methyl groups suggests that these groups are the cause of the dopant TL peaks. The SiO, filler exhibits catalytic effects and restricts the formation of methylene and methyl groups in the resin. EinfluP der thermischen Alterung auf die Thermolumineszenz eines EpoxidharzesBei der thermischen Alterung des Epoxidharzes Epidian-2 wurde eine Abnahme der Thermolumineszenz und eine Verringerung der energetischen Tiefe der Dotierungszentren gefunden. Aus der Korrelation zwischen der energetischen Tiefe der Thermolumineszenzzentren und dem Gehalt an Methyl-und Methylengruppen wird darauf geschlossen, da13 diese Gruppen die Ursache fur die Thermolumineszenzpeaks sind. Der SO,-Fullstoff hat einen katalytischen EinfluW und schrankt die Bildung von Methyl-und Methylengruppen in dem Harz cin. BnuRfiue mep&uztec?coeo cmapeuufi Ha mep&oAlo&ufiecyenyum ?co&noyndos eno~cu&oii CaoAbC npOqeCC TepMHqeCKOrO CTapeHIlFI 3IIOKCZiAHOt CMOJIbI Epidian-2 BbI3bIBaeT 3@@eKT 8aTyXaHHR H YMeHblUeHMR 3HepreTI4WXKOm my614~b1 qeHTpOB TepMOJIIOMliHeCqeH~kfH. CyWeCTByeT KOPpeJIFIqMFI MeXAy m y 6 1 4~o t QeHTpOB TepMOJIIoMElHeCqeHq&TK I4 KOJIHqeCTBOM MeTHJIOBbIX I4 MeTHJIeHOBbIX l'pynll 3 T 0 yKa3bIBaeT H a TO, 'IT0 OHI4 J%BJIXIOTC$i HCTOYHHKOM TepMOJIIOMHHeCqeHIJHH. HanOJIHHTeJIb sio2 np0FIBJIFIeT KaTaJIHTHYeCKBe CBOfiCTBa I4 OI'paHHWiBaeT 06pa30BaHUe MeTIXJIOBbIX I4 MeTIlJIeHOBblX rpynn.

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Effects of thermal ageing on thermoluminescence of an epoxy resin composition

Subocz

1989

Acta Polymerica

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Photoacoustic monitoring of adhesive curing

Torres-Filho

Perondi

Miranda

1988

J of Applied Polymer Sci

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The crosslinking reaction of an epoxy‐based resin has been monitored by observing the time evolution of the thermal diffusivity of the mixture, using photoacoustic spectroscopy. The results are interpreted in terms of the expected thermal properties of liquids, polymers and solids, and a comparison with the reported viscosity behavior in similar systems is also made. The potential of the technique for following the curing process is discussed.

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Thermoluminescence of the epoxy resin Epidian‐5

Abstract: Aus verarbeitungstechnischer Sicht wird ein Uberblick zur rheologischen Stoffcharakterisierung, insbesondere bei Verfestigungsprozessen, gegeben, in dessen Mittelpunkt der Phasenubergang flussig-fest steht.

Cited by 2 publications

References 4 publications

Effects of thermal ageing on thermoluminescence of an epoxy resin composition

Effects of thermal ageing on thermoluminescence of an epoxy resin composition

Photoacoustic monitoring of adhesive curing

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